Human Angiotensinogen enzyme-linked immunoassay kit

CAT: EH0239 Datasheet
Specification 96 Test
Sensitivity 0.25 ng/ml (10 μl)
Standard Curve Range 4.69~300 ng/ml
Standard Curve Gradient 7 Points
Number of Incubations 2
Detectable sample Liquid phase sample of soluble substances. For example: serum, plasma, cell culture supernatant, tissue grinding liquid, etc.
Sample Volume 10 μl
Type Fully Ready-to-Use
Operation Duration 120 min
ng/ml O.D. Average Corrected
0.00 0.0403 0.0513 0.0458
4.69 0.0701 0.0763 0.0732 0.0274
9.38 0.1047 0.1146 0.1097 0.0639
18.75 0.1803 0.1798 0.1801 0.1343
37.50 0.3458 0.3212 0.3335 0.2877
75.00 0.6617 0.6878 0.6748 0.6290
150.00 1.3420 1.1830 1.2625 1.2167
300.00 2.5350 2.7620 2.6485 2.6027

Precision

Intra-assay Precision Inter-assay Precision
Sample Number S1 S2 S3 S1 S2 S3
22 22 22 6 6 6
Average(ng/ml) 6.24 31.12 96.08 6.93 30.70 97.07
Standard Deviation 0.44 1.54 7.09 0.49 1.67 3.79
Coefficient of Variation(%) 7.1 5.0 7.4 7.1 5.4 3.9

Intra-assay Precision (Precision within an assay) Three samples of known concentration were tested twenty times on one plate to assess intra-assay precision.

Inter-assay Precision (Precision between assays) Three samples of known concentration were tested six times on one plate to assess intra-assay precision.

Spike Recovery

The spike recovery was evaluated by spiking 3 levels of human Angiotensinogen into health human serum sample. The un-spiked serum was used as blank in this experiment.
The recovery ranged from 86% to 120% with an overall mean recovery of 108%.

Sample Values

Sample Matrix Sample Evaluated Range (μg/ml) Detectable (%) Mean of Detectable (μg/ml)
Serum3029.69-62.05100.046.34

Serum/Plasma – Thirty samples from apparently healthy volunteers were evaluated for the presence of Angiotensinogen in this assay. No medical histories were available for the donors.

n.d. = non-detectable. Samples measured below the sensitivity are considered to be non-detectable.

Background: Angiotensinogen

Serpin A8 (serine proteinase inhibitor-clade A #8; also angiotensinogen/ANGT) is a secreted, 52-62 kDa glycoprotein member of the clade F-subfamily, serpin superfamily of protease inhibitors. It is expressed by neurons and hepatocytes, and undergoes extracellular cleavage by renin to create a ten amino acid (aa) peptide termed Ang/angiotensin I. This inactive peptide is further cleaved by ACE on the endothelial cell membrane to create bioactive Ang II. Ang II induces vascoconstriction and aldosterone release. Mature human angiotensinogen is 452 aa in length (aa 34-485). It contains Ang I (aa 34-43) that is cleaved to create Ang II (aa 34-41). Angiotensinogen may circulate in a 200 kDa complex with major basic protein (MBP), or as part of a larger 300 kDa complex with MBP and complement C3dg. Over aa 34-485, human serpin A8 shares 61% aa identity with mouse serpin A8.

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